摘要 i
Abstract ii
主目錄 iii
表目錄 vi
圖目錄 vii
第 1 章 前言 1
1.1 研究背景與動機 1
1.2 研究目的 3
第 2 章 文獻回顧 4
2.1 分子拓印技術 4
2.2 SPE應用 10
2.3 環境因子影響 14
2.3.1 pH 14
2.3.2 離子強度 18
2.3.3 天然有機物質 22
第 3 章 研究方法 26
3.1 實驗材料 28
3.2 MIH製備 30
3.3 材料特性鑑定 33
3.3.1 傅立葉轉換紅外線光譜分析 33
3.3.2 等溫氮氣吸脫附分析 33
3.3.3 熱重分析 33
3.3.4 表面電位分析 35
3.4 分析溶液配置 36
3.4.1 儲備液 36
3.4.2 檢量線溶液 36
3.4.3 混和溶液 36
3.4.4 酸鹼溶液 36
3.4.5 NaCl混合溶液 37
3.4.6 HA儲備液 37
3.4.7 環境水樣品處理與配置 38
3.5 吸附特性試驗 39
3.5.1 動力吸附 39
3.5.2 等溫吸附 40
3.5.3 溶劑影響 41
3.5.4 選擇性吸附 42
3.6 環境因子試驗 44
3.6.1 pH影響 44
3.6.2 離子強度影響 44
3.6.3 天然有機物質影響 45
3.7 SPE能力分析與比較 46
3.7.1 商用SPE材料吸附特性分析 46
3.7.2 SPE流程 47
3.7.3 分析方法建立 49
3.7.4 環境水樣分析與回收率 50
第 4 章 結果與討論 52
4.1 MIH材料鑑定 52
4.1.1 傅立葉轉換紅外線光譜分析 52
4.1.2 熱重分析 53
4.1.3 比表面積分析 55
4.2 MIH吸附特性 57
4.2.1 動力吸附 57
4.2.2 等溫吸附 59
4.2.3 溶劑影響 62
4.2.4 選擇性 65
4.3 環境因子影響 69
4.3.1 pH影響 69
4.3.2 離子強度影響 72
4.3.3 天然有機物質影響 73
4.4 SPE能力 75
4.4.1 商用SPE材料吸附特性 75
4.4.2 分析方法建立 77
4.4.3 環境水樣分析 79
第 5 章 結論與建議 82
5.1 結論 82
5.2 建議 84
參考文獻 85
附錄 95

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